I&EC Research: Industrial & Engineering Chemistry Research|2012

In-line Catalytic Purification of Carbon Dioxide Used in Precision Cleaning Applications

Michael E. Zorn | Dean T. Tompkins, John T. Etter, Marc A. Anderson, Walt A. Zeltner

The use of carbon dioxide (CO2) in precision cleaning applications requires a high-purity feed stream of CO2, which can add considerable cost to the overall process. The ability to purchase and clean a lower grade of CO2 would represent a significant cost savings. In this study, an in-line catalytic purification system was employed to clean two low-purity grades of CO2 to very low contaminant levels at flow rates relevant for full-scale precision cleaning applications (3.63 kg/h or 8 lb/h). A “food” grade of CO2 had an unpurified contaminant concentration of 4.0 ng/g, and a “bone dry” grade had an unpurified contaminant concentration of 4.9 ng/g. After catalytic purification, the food grade contaminant concentration was reduced to 0.14 ng/g (a 97% reduction), and the bone dry grade contaminant concentration was reduced to 0.26 ng/g (a 95% reduction).

DOI: 10.1021/ie202402w
Zorn, M.E., Tompkins, D.T., Zeltner, W.A., Anderson, M.A. and Etter, J.T. (2012) In-line catalytic purification of carbon dioxide used in precision cleaning applications, Ind. Eng. Chem. Res., 51, 2882-2887